Abstract:
A pressure vessel for single crystal growth using shrink fitting of the present invention comprises: a pressure vessel body manufactured by a heat-resistant alloy; a liner manufactured with a material having corrosion resistance and inserted into the pressure vessel body; and a lower part supporter inserted through the lower part of the pressure vessel body and supporting the lower part of the liner, wherein the liner is inserted into the pressure vessel body after the pressure vessel body is heated with a heating furnace.
Abstract:
본 발명은 단결정 성장 장치에 있어서, 원료 물질들을 배치하는 바스켓, 종자 결정들을 결속할 수 있는 랙 및 상기 바스켓과 상기 랙 사이에 위치하는 대류조절판을 포함하고, 상기 바스켓과 상기 랙이 분리되어 상기 대류조절판을 교체할 수 있는 것을 특징으로 하는 것을 특징으로 한다.
Abstract:
PURPOSE: A contact formation of silicon solar cells using conductive ink with nano-sized glass frit is provided to minimize the loss of electrode material and to reduce production costs. CONSTITUTION: An emitter layer(202) is formed on the upper part of a substrate. A reflection barrier layer is formed on the emitter layer. A first conductive layer(204) is patterned in the reflection barrier layer. A second conductive layer(205) is formed in the upper surface of the first conductive layer. A conductive ink composite is used in the process for forming the second conductive layer.
Abstract:
PURPOSE: Graphene and a manufacturing method of the same, a semiconductor device using the same, and a manufacturing method of the semiconductor are provided to control the electric characteristic of the graphene by generating the structural change of the graphene. CONSTITUTION: A manufacturing method of graphene controls the electric characteristic of graphene(104) by generating the structural change of the graphene. The structural change of the graphene is generated by doping nitrogen into the graphene based on nitrogen plasma treatment. The structural change of the graphene controls the electric characteristic of the graphene based on conductivity. The conductivity is controlled by the power of nitrogen plasma, the flux of nitrogen, the generating pressure of the nitrogen plasma, and the contact time of the nitrogen plasma and the graphene.
Abstract:
PURPOSE: A novel bismuth amino alkoxide compound with an amino alkoxide ligand and a method for preparing the same are provided to deposit a thin film or various alloys. CONSTITUTION: A bismuth amino alkoxide compound is denoted by chemical formula 1(Bi[O-A-NR^1R^2]_3) or formula 2(Bi[O-CR^3R^4(CH_2)_m-NR^1R^2]_3). A method for preparing the compound of chemical formula 1 comprises a step of reacting bismuth halide compound of chemical formula 2(BiX) with alkali metal salt of alcohol of chemical formula 4(M[O-A-NR_1R_2]). A bismuth compound of chemical formula 6(Bi[NR^5_2]_3) is prepared by reacting a bismuth halide compound of chemical formula 3(BiX_3) with alkali metal compounds of chemical formula 5(M[NR^5_2]). A bismuth-containing thin film is prepared using the bismuth amino alkoxide compounds as a precursor.
Abstract:
PURPOSE: A method for manufacturing a thin film transistor using a two-dimensional graphene nano ribbon is provided to control the length of a graphene nano ribbon by using a Pd catalyst. CONSTITUTION: A source electrode and a drain electrode are connected to both sides of a channel layer. A gate electrode corresponds to the channel layer. A gate insulation layer is formed between the channel layer and the gate electrode. After the gate insulation layer is deposited on the gate electrode, the source electrode and the drain electrode are formed by a lithograph process. A hydrophobic organic layer is laminated after the gate insulation layer, the source electrode, and the drain electrode are surface-processed.
Abstract:
본 발명은 파라-디옥사논(p-dioxanone)을 정제하는 방법에 관한 것으로, (1) 파라-디옥사논을 냉각시켜 파라-디옥사논을 결정화시키는 단계; (2) 결정화된 파라-디옥사논을 파쇄하고 여과시키는 단계; (3) 여과된 파라-디옥사논 입자를 고진공하에서 파라-디옥사논의 녹는점 이하의 온도에서 건조시키는 단계; 및 (4) 건조된 파라-디옥사논을 열-용융시킨 후 감압하에서 증류하는 단계를 포함하는, 본 발명의 파라-디옥사논의 정제방법에 따르면 99.9% 이상의 고순도 파라-디옥사논을 높은 수율로 간단하게 수득할 수 있다.
Abstract:
본 발명은 N-알킬몰포리논의 제조방법에 관한 것으로, 반응 초기에 2-p-디옥사논 또는 이의 중합체와 1급 알킬아민을 수성 매질 중에서 1:0.8∼1.1의 몰비로 반응시키고, 반응용액에 상기 1급 알킬아민의 수용액을 불활성 기체와 함께 추가로 공급하면서 열린 반응계에서 반응을 진행하는 것을 특징으로 하며, 이러한 본 발명의 방법에 의하면, 짧은 시간 내에 N-알킬몰포리논을 고선택성 및 고수율로 제조할 수 있다.
Abstract:
PURPOSE: Provided are a composite metal oxide catalyst for vapour phase hydrogenation, a preparation method thereof and a method for preparing phthalide from ester phthalate using the composite metal oxide catalyst, wherein the catalyst exhibits high selectivity, productivity and extended catalytic activity in the process of preparing phthalide from ester phthalate by vapour phase hydrogenation even under the mild conditions of low temperature at 130 to 220 deg.C, low pressure of 1 to 10 atm and low hydrogen/ester phthalate ratio ranging from 500 to 3,000. CONSTITUTION: The catalyst is represented as follows: £CuO(a)ZnO(b)MnO2(c)SiO2(d)|(100-x)M(x), where M is at least one oxide selected from the group consisting of Re oxides, Ru oxides and Ag oxides, a is 20 to 90, b is 0.01 to 10, c is 0.01 to 5, d is 5 to 65 and x is 0.001 to 5, wherein a, b, c, d and x are expressed on the basis of weight. The preparation method of the catalyst comprises the steps of preparing a mixed solution containing copper salt, zinc salt and manganese salt; adding an alkali solution to the mixed solution to coprecipitate copper, zinc and manganese in the form of hydrogel, wherein the temperature of the mixed solution is in the range of 1 to 30 deg.C and pH is kept in the range of 6 to 9; adding nano size colloidal silica to the hydrogel, thereby obtaining a mixed slurry, wherein the colloidal silica is stabilized by NH4¬+, Na¬+ and other alkali metal, and particle size and specific surface area thereof are 4 to 60 nm and 100 to 300 m¬2/g, respectively; hydrothermal aging the mixed slurry at 50 to 100 deg.C for more than 0.5 hr; filtering the mixed slurry after hydrothermal aging to separate cake, followed by washing the cake, wherein the washing is conducted until residual concentration of alkali metal is less than 1000 ppm; and drying and tableting the washed cake.